1,2,3,4-Tetrachlorohexafluorobutane

Base Information

• Chemical Name: 1,2,3,4-Tetrachlorohexafluorobutane
• CAS No.: 375-45-1
• Molecular Formula: C4Cl4 F6
• Molecular Weight: 303.846
• Hs Code.: 2903799090
• European Community (EC) Number: 609-441-9
• DSSTox Substance ID: DTXSID40339866
• Nikkaji Number: J104.117G
• ChEMBL ID: CHEMBL452940
• Mol file: 375-45-1.mol

Synonyms:1,2,3,4-Tetrachlorohexafluorobutane;375-45-1;Hexafluoro-1,2,3,4-tetrachlorobutane;1,2,3,4-Tetrachloro-1,1,2,3,4,4-hexafluorobutane;MFCD00040135;28107-59-7;Butane, 1,2,3,4-tetrachloro-1,1,2,3,4,4-hexafluoro-;Butane, 1,2,3,4-tetrachlorohexafluoro-;bisMPA dendrimer;EINECS 248-847-7;SCHEMBL710882;CHEMBL452940;DTXSID40339866;1,2,3,4-tetrachlorohexafluoro-butane;AKOS015852656;BS-25118;FT-0626976;EC 938-148-1;A823748;1,2,3,4-Tetrachloro-1,1,2,3,4,4-hexafluorobutane #

Chemical Property of 1,2,3,4-Tetrachlorohexafluorobutane

Chemical Property:

• Boiling Point: 131.5°Cat760mmHg
• Flash Point: 47.9°C
• PSA: 0.00000
• Density: 1.756g/cm³
• LogP: 4.45880
• XLogP3: 4.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 3
• Exact Mass: 303.862880
• Heavy Atom Count: 14
• Complexity: 210

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(C(C(F)(F)Cl)(F)Cl)(C(F)(F)Cl)(F)Cl

Technology Process of 1,2,3,4-Tetrachlorohexafluorobutane

There total 35 articles about 1,2,3,4-Tetrachlorohexafluorobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1,2-dichloro-1,2,2-trifluoro-1-iodoethane (354-61-0) → perfluoro-1,2,3,4-tetrachlorobutane (375-45-1)

Guidance literature:

With zinc; at 40 ℃; for 20h; Temperature; Concentration; Ionic liquid; Large scale;

Reference yield: 91.0%

1,2-dihydro-2-iodo-1,1,2-trifluoroethane → perfluoro-1,2,3,4-tetrachlorobutane (375-45-1)

Guidance literature:

With zirconium oxide; ethyl acetate; zinc; for 16h; Reagent/catalyst;

Reference yield: 87.0%

1,2,3,4-tetrafluoro-1,1,2,3,4,4-hexachlorobutane (375-43-9) → perfluoro-1,2,3,4-tetrachlorobutane (375-45-1)

Guidance literature:

With tetramethylammonium fluoride; In diethylene glycol dimethyl ether; at 80 ℃; for 6h; Reagent/catalyst; Temperature;

upstream raw materials:

dichloromethane

1,2-dichloro-1,2,2-trifluoro-1-iodoethane

1,2-dichloro-1,2-difluoroethene

1,1,2,3,4,4-hexafluorobutane

Downstream raw materials:

hexafluoro-1,3-butadiene

(E)-1,4-dichloro-1,1,2,3,4,4-hexafluorobut-2-ene

(Z)-1,4-dichloro-1,1,2,3,4,4-hexafluorobut-2-ene

1,1,2,3,4,4-hexafluoro-but-2-ene

Refernces

• 1、 -. "Preparation method of hexafluorobutadiene". Paragraph 0039; 0048; 0049; 0052; 0060; 0061; 0064; 0072. . Retrieved 2021/01/29.
• 2、 -. "METHOD AND APPARATUS FOR PRODUCING FLUORINE-CONTAINING ORGANIC COMPOUND". Paragraph 0057-0067. . Retrieved 2020/12/01.