C₄₁H₃₉NO₇

Base Information

• Chemical Name: C₄₁H₃₉NO₇
• CAS No.: 1221269-86-8
• Molecular Formula: C₄₁H₃₉NO₇
• Molecular Weight: 657.763
• Mol file: 1221269-86-8.mol

Synonyms:C₄₁H₃₉NO₇

Chemical Property of C₄₁H₃₉NO₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₁H₃₉NO₇

There total 6 articles about C₄₁H₃₉NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

C32H31NO4 (1221269-84-6) + 4-iodo-2,5-dimethoxybenzenecarbaldehyde (90064-47-4) → C41H39NO7 (1221269-86-8)

Guidance literature:

With trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); sodium carbonate; In N,N-dimethyl acetamide; at 130 ℃; for 24h;

DOI:10.1039/b917065k

Reference yield:

2,5-dimethoxybenzaldehyde (93-02-7) → C41H39NO7 (1221269-86-8)

Guidance literature:

Multi-step reaction with 6 steps

1: iodine; silver nitrate / methanol / 7 h / 20 °C

2: copper(I) oxide / N,N-dimethyl acetamide / 72 h / 190 °C

3: potassium tert-butylate; methyl-triphenylphosphonium iodide / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

4: trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); 2,6-di-tert-butyl-4-methyl-phenol; sodium carbonate / tetrahydrofuran / 24 h / 110 °C

5: potassium tert-butylate; methyl-triphenylphosphonium iodide / tetrahydrofuran / 4 h / 20 °C

6: trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); sodium carbonate / N,N-dimethyl acetamide / 24 h / 130 °C

With copper(I) oxide; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); 2,6-di-tert-butyl-4-methyl-phenol; potassium tert-butylate; iodine; methyl-triphenylphosphonium iodide; sodium carbonate; silver nitrate; In tetrahydrofuran; methanol; N,N-dimethyl acetamide;

DOI:10.1039/b917065k

Reference yield:

4-iodo-2,5-dimethoxybenzenecarbaldehyde (90064-47-4) → C41H39NO7 (1221269-86-8)

Guidance literature:

Multi-step reaction with 5 steps

1: copper(I) oxide / N,N-dimethyl acetamide / 72 h / 190 °C

2: potassium tert-butylate; methyl-triphenylphosphonium iodide / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

3: trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); 2,6-di-tert-butyl-4-methyl-phenol; sodium carbonate / tetrahydrofuran / 24 h / 110 °C

4: potassium tert-butylate; methyl-triphenylphosphonium iodide / tetrahydrofuran / 4 h / 20 °C

5: trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); sodium carbonate / N,N-dimethyl acetamide / 24 h / 130 °C

With copper(I) oxide; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); 2,6-di-tert-butyl-4-methyl-phenol; potassium tert-butylate; methyl-triphenylphosphonium iodide; sodium carbonate; In tetrahydrofuran; N,N-dimethyl acetamide;

DOI:10.1039/b917065k

upstream raw materials:

C₂₁H₁₉NO₃

2,5-dimethoxy-N,N'-diphenyl-4-vinylaniline

C₃₁H₂₉NO₅

C₃₂H₃₁NO₄

Downstream raw materials:

C₄₄H₄₀N₂O₈

Refernces