benzyltrineopentoxyphosphonium trifluoromethanesulfonate

Base Information

• Chemical Name: benzyltrineopentoxyphosphonium trifluoromethanesulfonate
• CAS No.: 123750-96-9
• Molecular Formula: CF₃O₃S*C₂₂H₄₀O₃P
• Molecular Weight: 532.602
• Mol file: 123750-96-9.mol

Synonyms:benzyltrineopentoxyphosphonium trifluoromethanesulfonate

Chemical Property of benzyltrineopentoxyphosphonium trifluoromethanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of benzyltrineopentoxyphosphonium trifluoromethanesulfonate

There total 3 articles about benzyltrineopentoxyphosphonium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2-dimethyl-propanol-1 (75-84-3) → benzyltrineopentoxyphosphonium trifluoromethanesulfonate (123750-96-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / phosphorus trichloride, pyridine / petroleum ether / 0.67 h / 0 - 25 °C

2: CCl₄ / 1.) -20 deg C, 30 min, 2.) RT, 30 min

With pyridine; phosphorus trichloride; In tetrachloromethane; Petroleum ether;

DOI:10.1021/ja00006a049

Reference yield:

benzyl alcohol (100-51-6,185532-71-2) → benzyltrineopentoxyphosphonium trifluoromethanesulfonate (123750-96-9)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / CCl₄ / 0.5 h / -20 °C

2: CCl₄ / 1.) -20 deg C, 30 min, 2.) RT, 30 min

With pyridine; In tetrachloromethane;

DOI:10.1021/ja00006a049

Reference yield:

trineopentyl phosphite (14540-52-4) + benzyl triflate (17674-16-7) → benzyltrineopentoxyphosphonium trifluoromethanesulfonate (123750-96-9)

Guidance literature:

In tetrachloromethane; Yield given; 1.) -20 deg C, 30 min, 2.) RT, 30 min;

DOI:10.1021/ja00006a049

upstream raw materials:

trineopentyl phosphite

benzyl triflate

2,2-dimethyl-propanol-1

benzyl alcohol

Downstream raw materials:

trineopentyl phosphite

Benzyl-phosphonic acid bis-(2,2-dimethyl-propyl) ester

toluene

Refernces