Technology Process of C18H19NO2S2
There total 3 articles about C18H19NO2S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 15h;
DOI:10.1021/op500031z
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium carbonate; [2,2]bipyridinyl; oxygen; copper diacetate / acetonitrile / 20 - 55 °C / Inert atmosphere
2: potassium carbonate / N,N-dimethyl-formamide / 15 h / 20 °C
With
[2,2]bipyridinyl; oxygen; copper diacetate; sodium carbonate; potassium carbonate;
In
N,N-dimethyl-formamide; acetonitrile;
1: |Chan-Lam Coupling;
DOI:10.1021/op500031z
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: toluene / 0.25 h / 0 - 15 °C / Inert atmosphere
1.2: 5 - 25 °C / Inert atmosphere
1.3: 4 h / 20 - 25 °C / Inert atmosphere
2.1: sodium carbonate; [2,2]bipyridinyl; oxygen; copper diacetate / acetonitrile / 20 - 55 °C / Inert atmosphere
3.1: potassium carbonate / N,N-dimethyl-formamide / 15 h / 20 °C
With
[2,2]bipyridinyl; oxygen; copper diacetate; sodium carbonate; potassium carbonate;
In
N,N-dimethyl-formamide; toluene; acetonitrile;
2.1: |Chan-Lam Coupling;
DOI:10.1021/op500031z