3-nitro-2,4-diphenylpyridine

Base Information

• Chemical Name: 3-nitro-2,4-diphenylpyridine
• CAS No.: 1335110-51-4
• Molecular Formula: C₁₇H₁₂N₂O₂
• Molecular Weight: 276.294
• Mol file: 1335110-51-4.mol

Synonyms:3-nitro-2,4-diphenylpyridine

Chemical Property of 3-nitro-2,4-diphenylpyridine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-nitro-2,4-diphenylpyridine

There total 2 articles about 3-nitro-2,4-diphenylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

bromobenzene (108-86-1,52753-63-6) + 2-phenyl-3-nitropyridine (134896-35-8) → 3-nitro-2,4-diphenylpyridine (1335110-51-4) + 3-nitro-2,4,5-triphenylpyridine (1335110-63-8)

Guidance literature:

With palladium diacetate; caesium carbonate; trimethylpyruvic acid; silver carbonate; di(1-adamantyl)-N-butylphosphine hydroiodide; In toluene; at 120 ℃; for 22h; regioselective reaction; Inert atmosphere;

DOI:10.1021/ja206022p

Reference yield: 75.0%

3-nitropyridine (2530-26-9) + bromobenzene (108-86-1,52753-63-6) → 3-nitro-2,4-diphenylpyridine (1335110-51-4) + 4-phenyl-3-nitropyridine (220952-00-1)

Guidance literature:

With palladium diacetate; caesium carbonate; trimethylpyruvic acid; silver carbonate; di(1-adamantyl)-N-butylphosphine hydroiodide; In toluene; at 120 ℃; for 22h; regioselective reaction; Inert atmosphere;

DOI:10.1021/ja206022p

upstream raw materials:

3-nitropyridine

bromobenzene

2-phenyl-3-nitropyridine

Refernces