ETHYL 2-AMINO-2-CYANOACETATE OXALATE H2O

Base Information

• Chemical Name: ETHYL 2-AMINO-2-CYANOACETATE OXALATE H2O
• CAS No.: 32683-02-6
• Molecular Formula: C5H8N2O2
• Molecular Weight: 128.131
• Hs Code.: 2926909090
• Mol file: 32683-02-6.mol

Synonyms:Aceticacid, aminocyano-, ethyl ester (9CI);Glycine, 2-cyano-, ethyl ester (8CI);(Amino)(cyano)acetic acid ethyl ester;2-Amino-2-cyanoacetic acid ethyl ester;Ethyl 2-amino-2-cyanoacetate;Ethyl aminocyanoacetate;Ethyl a-amino-a-cyanoacetate;

Chemical Property of ETHYL 2-AMINO-2-CYANOACETATE OXALATE H2O

Chemical Property:

• Vapor Pressure: 0.286mmHg at 25°C
• Refractive Index: 1.455
• Boiling Point: 202.9 °C at 760 mmHg
• PKA: 2.82±0.50(Predicted)
• Flash Point: 76.5 °C
• PSA: 76.11000
• Density: 1.144 g/cm³
• LogP: 0.10068
• Storage Temp.: Keep in dark place,Sealed in dry,Store in freezer, under -20°C

Purity/Quality:

99%, ^*data from raw suppliers

Ethyl2-amino-2-cyanoacetate 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ETHYL 2-AMINO-2-CYANOACETATE OXALATE H2O

There total 1 articles about ETHYL 2-AMINO-2-CYANOACETATE OXALATE H2O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl phenylazocyanoacetate (5335-36-4) → aniline (62-53-3) + ethyl-2-aminocyano acetate (32683-02-6)

Guidance literature:

With potassium chloride; cetyltrimethylammonim bromide; In methanol; at 30 ℃; Mechanism; polarographic reduction at pH=6.0 (Britton-Robinson buffer);

Reference yield: 87.0%

phenyl isocyanate (103-71-9) + ethyl-2-aminocyano acetate (32683-02-6) → 5-amino-4-ethoxycarbonyl-1-phenylimidazol-2-one

Guidance literature:

With triethylamine; In 1,2-dichloro-ethane; for 1h; Heating;

DOI:10.1016/j.tetlet.2004.01.088

Reference yield: 84.0%

2,6-difluorobenzoylchloride (18063-02-0) + ethyl-2-aminocyano acetate (32683-02-6) → N-(1-cyano-2-ethylperoxyethyl)-2,6-difluorobenzamide (1187056-39-8)

Guidance literature:

With pyridine; In dichloromethane; at 0 - 20 ℃;

upstream raw materials:

ethyl phenylazocyanoacetate

Downstream raw materials:

ethyl 2-acetamido-2-cyanoacetate

ethyl 5-amino-2-(phenylamino)thiazole-4-carboxylate

5-amino-2-methylamino-thiazole-4-carboxylic acid ethyl ester

5-amino-2-benzoylamino-thiazole-4-carboxylic acid ethyl ester

Refernces