ETHYL HEPTAFLUOROBUTYRYLACETATE

Base Information

• Chemical Name: ETHYL HEPTAFLUOROBUTYRYLACETATE
• CAS No.: 336-62-9
• Molecular Formula: C8H7 F7 O3
• Molecular Weight: 284.131
• Hs Code.: 2918300090
• Mol file: 336-62-9.mol

Synonyms:Ethyl4,4,5,5,6,6,6-heptafluoro-3-oxohexanoate

Chemical Property of ETHYL HEPTAFLUOROBUTYRYLACETATE

Chemical Property:

• Refractive Index: 1.36
• Boiling Point: 170.1°Cat760mmHg
• PKA: 7.78±0.46(Predicted)
• Flash Point: 55.6°C
• PSA: 43.37000
• Density: 1.424g/cm³
• LogP: 2.34160

Purity/Quality:

98%min ^*data from raw suppliers

Ethyl heptafluorobutyrylacetate 97% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi,F
• Statements: 10
• Safety Statements: 16

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ETHYL HEPTAFLUOROBUTYRYLACETATE

There total 2 articles about ETHYL HEPTAFLUOROBUTYRYLACETATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Acetyl-4,4,5,5,6,6,6-heptafluoro-3-oxo-hexanoic acid ethyl ester (115479-06-6) → (2,2,3,3,4,4,4-heptafluorobutanoyl)acetic acid ethyl ester (336-62-9) + ethyl acetoacetate (141-97-9)

Guidance literature:

With potassium hydroxide; In ethanol; Product distribution; other reagent, solvent;

DOI:10.1007/BF00958359

Reference yield:

2-Acetyl-4,4,5,5,6,6,6-heptafluoro-3-oxo-hexanoic acid ethyl ester (115479-06-6) → 5,5,6,6,7,7,7-heptafluoro-heptane-2,4-dione (356-30-9) + (2,2,3,3,4,4,4-heptafluorobutanoyl)acetic acid ethyl ester (336-62-9)

Guidance literature:

With water; Product distribution; Heating; other reagent;

DOI:10.1007/BF00958359

Reference yield: 76.0%

(2,2,3,3,4,4,4-heptafluorobutanoyl)acetic acid ethyl ester (336-62-9) + 1-chloro-1-(phenylhydrazono)propanone (18440-58-9,1017827-91-6) → 4-ethoxycarbonyl-5-(heptafluoro-n-propyl)-3-methylcarbonyl-1-phenylpyrazole

Guidance literature:

With triethylamine; In benzene; Heating;

DOI:10.1016/S0040-4020(01)85356-4

upstream raw materials:

2-Acetyl-4,4,5,5,6,6,6-heptafluoro-3-oxo-hexanoic acid ethyl ester

Downstream raw materials:

heptafluoropropyl methyl ketone

Ethyl (Z)-4,4,5,5,6,6,6-heptafluoro-3-benzylamino-2-hexenoate

ethyl 4,4,5,5,6,6,6-heptafluoro-3-oxo-2-(triphenyl-λ⁵-phosphanylidenehydrazono)hexanoate

4,4,5,5,6,6,6-Heptafluoro-3-{[1-phenyl-meth-(E)-ylidene]-amino}-hexanoic acid ethyl ester

Refernces