Technology Process of 1-Aminocyclohexanphosphonsaeure-di-i-propylester
There total 4 articles about 1-Aminocyclohexanphosphonsaeure-di-i-propylester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
ethanol;
at 20 ℃;
for 3h;
under 750.06 Torr;
DOI:10.1080/00397919608004650
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) BuLi / 1.) THF, -78 deg C, 30 min, 2.) THF, -78 deg C, 1 h
2: tetrahydrofuran; acetic acid / 3 h / Ambient temperature
3: 64 percent / H2 / Pd/C / ethanol / 3 h / 20 °C / 750.06 Torr
With
n-butyllithium; hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol; acetic acid;
DOI:10.1080/00397919608004650
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrahydrofuran; acetic acid / 3 h / Ambient temperature
2: 64 percent / H2 / Pd/C / ethanol / 3 h / 20 °C / 750.06 Torr
With
hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol; acetic acid;
DOI:10.1080/00397919608004650
