4-methylcycloheptanone

Base Information

• Chemical Name: 4-methylcycloheptanone
• CAS No.: 5452-36-8
• Molecular Formula: C8H14 O
• Molecular Weight: 126.1962
• Mol file: 5452-36-8.mol

Synonyms:4-Methylcycloheptanone;NSC 18963

Chemical Property of 4-methylcycloheptanone

Chemical Property:

• Vapor Pressure: 0.716mmHg at 25°C
• Boiling Point: 184.9°C at 760 mmHg
• Flash Point: 58.6°C
• Density: 0.897g/cm³

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-methylcycloheptanone

There total 15 articles about 4-methylcycloheptanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+/-)-cis-8,8-dibromobicyclo<5.1.0>oct-2-en-4-one (98875-51-5) → 4-methyl-cycloheptanone (5452-36-8)

Guidance literature:

With hydrogen; sodium acetate; palladium on activated charcoal; In ethanol;

DOI:10.1039/j39670000358

Reference yield:

4-methyl-2,4,6-cycloheptatrien-1-one (1654-62-2) → 4-methyl-cycloheptanone (5452-36-8)

Guidance literature:

With hydrogen; palladium;

DOI:10.1007/BF00914980

Reference yield:

→ 4-methyl-cycloheptanone (5452-36-8)

Guidance literature:

With iron; at 300 - 350 ℃;

upstream raw materials:

diazomethane

1-methylcyclohexan-4-one

1-Aminomethyl-4-methyl-cyclohexanol

optically inactive 4-hydroxy-1-methyl-cycloheptane

Downstream raw materials:

1-Methyl-4-methylene-cycloheptane

Refernces

• 1、 Zbiral,E. et al.. "-". . p. 1155 - 1166. Retrieved 1961.