9-(2-propynyl)-β-ionyl acetate

Base Information Edit

Chemical Name:9-(2-propynyl)-β-ionyl acetate
CAS No.:74352-12-8
Molecular Formula:C₁₈H₂₆O₂
Molecular Weight:274.403
Hs Code.:
Mol file:74352-12-8.mol

Synonyms:9-(2-propynyl)-β-ionyl acetate

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Chemical Property of 9-(2-propynyl)-β-ionyl acetate Edit

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Technology Process of 9-(2-propynyl)-β-ionyl acetate

There total 2 articles about 9-(2-propynyl)-β-ionyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 74352-11-7
6-(2-methyl-6,6-dimethylcyclohex-1-en-1-yl)-3-methylhex-1-ene-5-yne-3-ol

: 108-24-7
acetic anhydride

: 74352-12-8
9-(2-propynyl)-β-ionyl acetate

Guidance literature:: With dmap; In toluene;
DOI:10.1021/ja00536a046

Reference yield:

: 79-77-6,14901-07-6
(E)-β-ionone

: 74352-12-8
9-(2-propynyl)-β-ionyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Mg / 1.) HgCl₂ / 1.) ether, 30 min, 2.) ether, 45 min

2: 90 percent / DMAP / toluene / 1 h / Ambient temperature

With dmap; magnesium; mercury dichloride; In toluene;