1,2,3,4,6,7,8,9,10,10,11,11-Dodecachloro-1,4,4a,5a,6,9,9a,9b-octahydro-1,4:6,9-dimethanodibenzofuran

Base Information

• Chemical Name: 1,2,3,4,6,7,8,9,10,10,11,11-Dodecachloro-1,4,4a,5a,6,9,9a,9b-octahydro-1,4:6,9-dimethanodibenzofuran
• CAS No.: 31107-44-5
• Deprecated CAS: 56449-79-7,1482458-42-3
• Molecular Formula: C14H4Cl12O
• Molecular Weight: 613.621
• Hs Code.: 29038900
• European Community (EC) Number: 250-472-9
• Nikkaji Number: J68.889D
• Mol file: 31107-44-5.mol

Synonyms:dechlorane 602

Chemical Property of 1,2,3,4,6,7,8,9,10,10,11,11-Dodecachloro-1,4,4a,5a,6,9,9a,9b-octahydro-1,4:6,9-dimethanodibenzofuran

Chemical Property:

• Vapor Pressure: 1.11E-11mmHg at 25°C
• Melting Point: 296-298oC
• Refractive Index: 1.696
• Boiling Point: 552.3 °C at 760 mmHg
• Flash Point: 177.9 °C
• PSA: 9.23000
• Density: 2.04 g/cm³
• LogP: 7.67720
• Storage Temp.: Amber Vial, Refrigerator
• Solubility.: Chloroform (Slightly, Heated), Ethyl Acetate (Slightly)
• XLogP3: 6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 613.643597
• Heavy Atom Count: 27
• Complexity: 811

Purity/Quality:

98%Min ^*data from raw suppliers

Dechlorane 602 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C12C3C(C4(C(=C(C3(C4(Cl)Cl)Cl)Cl)Cl)Cl)OC1C5(C(=C(C2(C5(Cl)Cl)Cl)Cl)Cl)Cl

Technology Process of 1,2,3,4,6,7,8,9,10,10,11,11-Dodecachloro-1,4,4a,5a,6,9,9a,9b-octahydro-1,4:6,9-dimethanodibenzofuran

There total 1 articles about 1,2,3,4,6,7,8,9,10,10,11,11-Dodecachloro-1,4,4a,5a,6,9,9a,9b-octahydro-1,4:6,9-dimethanodibenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

furan (110-00-9) + hexachlorocyclopentadiene (77-47-4) → 1,2,3,4,6,7,8,9,10,10,11,11-dodecachloro-1,4,4a,5a,6,9,9a,9b-octahydro-1,4,6,9-dimethanodibenzofuran 4 (31107-44-5)

Guidance literature:

at 135 - 140 ℃; for 4h;

upstream raw materials:

furan

hexachlorocyclopentadiene

Refernces