C₁₃H₁₇NO₂

Base Information

• Chemical Name: C₁₃H₁₇NO₂
• CAS No.: 1015076-72-8
• Molecular Formula: C₁₃H₁₇NO₂
• Molecular Weight: 219.283
• Mol file: 1015076-72-8.mol

Synonyms:C₁₃H₁₇NO₂

Chemical Property of C₁₃H₁₇NO₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₃H₁₇NO₂

There total 1 articles about C₁₃H₁₇NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

C14H17NO3 (1015076-70-6) → C13H17NO2 (1015076-72-8)

Guidance literature:

C₁₄H₁₇NO₃; With lithium aluminium tetrahydride; In tetrahydrofuran; tert-butyl alcohol; at 0 - 50 ℃;

With hydrogenchloride; water; In tetrahydrofuran; tert-butyl alcohol;

Reference yield: 100.0%

C13H17NO2 (1015076-72-8) + methanesulfonyl chloride (124-63-0) → C14H19NO4S (1015076-73-9)

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃; for 3.25h;

Reference yield:

C13H17NO2 (1015076-72-8) → C15H19NO2S (1015076-74-0)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 3.25 h / 0 °C

2: caesium carbonate / methanol; N,N-dimethyl-formamide / 20 °C

With caesium carbonate; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;

upstream raw materials:

C₁₄H₁₇NO₃

Downstream raw materials:

C₁₄H₁₉NO₄S

C₁₅H₁₉NO₂S

Refernces