Technology Process of C30H37N7O7S
There total 7 articles about C30H37N7O7S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 100 percent / Et3N / CH2Cl2 / 0 - 20 °C
2.1: s-BuLi; TMEDA / diethyl ether / -90 °C
2.2: 35 percent / diethyl ether / -90 - 20 °C
3.1: 99 percent / HCl / ethyl acetate / 0 - 20 °C
4.1: 100 percent / HCl / ethyl acetate / 20 °C
5.1: 86 percent / Et3N / CH2Cl2 / 0 °C
With
hydrogenchloride; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; triethylamine;
In
diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1016/S0960-894X(01)00351-1
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: s-BuLi; TMEDA / diethyl ether / -90 °C
1.2: 35 percent / diethyl ether / -90 - 20 °C
2.1: 99 percent / HCl / ethyl acetate / 0 - 20 °C
3.1: 100 percent / HCl / ethyl acetate / 20 °C
4.1: 86 percent / Et3N / CH2Cl2 / 0 °C
With
hydrogenchloride; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; triethylamine;
In
diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1016/S0960-894X(01)00351-1
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Et3N / -35 °C
2: 100 percent / HCl / ethyl acetate / 20 °C
3: 86 percent / Et3N / CH2Cl2 / 0 °C
With
hydrogenchloride; triethylamine;
In
dichloromethane; ethyl acetate;
DOI:10.1016/S0960-894X(01)00351-1