C₁₄H₁₁N₃OS₂

Base Information

• Chemical Name: C₁₄H₁₁N₃OS₂
• CAS No.: 1430235-98-5
• Molecular Formula: C₁₄H₁₁N₃OS₂
• Molecular Weight: 301.393
• Mol file: 1430235-98-5.mol

Synonyms:C₁₄H₁₁N₃OS₂

Chemical Property of C₁₄H₁₁N₃OS₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₁₁N₃OS₂

There total 1 articles about C₁₄H₁₁N₃OS₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-benzylsulfanylnicotinic acid (112811-90-2) → C14H11N3OS2 (1430235-98-5)

Guidance literature:

Multi-step reaction with 3 steps

1: sulfuric acid / 10 h / Reflux

2: hydrazine hydrate / methanol / 5 h / Reflux

3: carbon disulfide; potassium hydroxide / methanol / 5 h / Reflux

With carbon disulfide; hydrazine hydrate; sulfuric acid; potassium hydroxide; In methanol;

DOI:10.1016/j.ejmech.2012.12.055

Reference yield: 72.0%

N-(5-methylthiazol-2-yl)-2-chloroacetamide + C14H11N3OS2 (1430235-98-5) → C20H17N5O2S3 (1430235-99-6)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 8h;

DOI:10.1016/j.ejmech.2012.12.055

Reference yield: 69.0%

C4H5ClN4O (137141-14-1) + C14H11N3OS2 (1430235-98-5) → C18H15N7O2S2 (1430236-02-4)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 10h;

DOI:10.1016/j.ejmech.2012.12.055

upstream raw materials:

2-benzylsulfanylnicotinic acid

Downstream raw materials:

C₂₀H₁₇N₅O₂S₃

C₂₂H₂₀N₆O₄S₂

C₂₀H₁₄Cl₂N₆O₂S₂

C₁₈H₁₅N₇O₂S₂

Refernces