N-trifluoromethylsulfonyl-S-trifluoromethyl-S-p-aminophenylsulfoximide

Base Information

• Chemical Name: N-trifluoromethylsulfonyl-S-trifluoromethyl-S-p-aminophenylsulfoximide
• CAS No.: 109139-25-5
• Molecular Formula: C₈H₆F₆N₂O₃S₂
• Molecular Weight: 356.27
• Mol file: 109139-25-5.mol

Synonyms:N-trifluoromethylsulfonyl-S-trifluoromethyl-S-p-aminophenylsulfoximide

Chemical Property of N-trifluoromethylsulfonyl-S-trifluoromethyl-S-p-aminophenylsulfoximide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-trifluoromethylsulfonyl-S-trifluoromethyl-S-p-aminophenylsulfoximide

There total 3 articles about N-trifluoromethylsulfonyl-S-trifluoromethyl-S-p-aminophenylsulfoximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

C8H4F6N2O5S2 (109139-24-4) → N-trifluoromethylsulfonyl-S-trifluoromethyl-S-p-aminophenylsulfoximide (109139-25-5)

Guidance literature:

With hydrogenchloride; iron; In methanol; at 70 ℃; for 2h;

Reference yield:

C7H4F3N2O3S(1-)*Na(1+) → N-trifluoromethylsulfonyl-S-trifluoromethyl-S-p-aminophenylsulfoximide (109139-25-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 43 percent / acetonitrile / 3 h / 80 °C / glass tube

2: 81 percent / Fe powder, conc. hydrochloric acid / methanol / 2 h / 70 °C

With hydrogenchloride; iron; In methanol; acetonitrile;

Reference yield:

imino(4-nitrophenyl)(trifluoromethyl)-λ6-sulfanone (95448-39-8) → N-trifluoromethylsulfonyl-S-trifluoromethyl-S-p-aminophenylsulfoximide (109139-25-5)

Guidance literature:

Multi-step reaction with 3 steps

1: NaH / diethyl ether / 2 h

2: 43 percent / acetonitrile / 3 h / 80 °C / glass tube

3: 81 percent / Fe powder, conc. hydrochloric acid / methanol / 2 h / 70 °C

With hydrogenchloride; iron; sodium hydride; In methanol; diethyl ether; acetonitrile;

upstream raw materials:

C₈H₄F₆N₂O₅S₂

imino(4-nitrophenyl)(trifluoromethyl)-λ⁶-sulfanone

Downstream raw materials:

N-trifluoromethylsulfonyl-S-trifluoromethyl-S-p-(4-dimethylaminophenylazo)phenylsulfoximide

Refernces