butyl 3-(2-benzoylbenzofuran-3-yl)-2-methylpropanoate

Base Information

• Chemical Name: butyl 3-(2-benzoylbenzofuran-3-yl)-2-methylpropanoate
• CAS No.: 1638610-40-8
• Molecular Formula: C₂₃H₂₄O₄
• Molecular Weight: 364.441
• Mol file: 1638610-40-8.mol

Synonyms:butyl 3-(2-benzoylbenzofuran-3-yl)-2-methylpropanoate

Chemical Property of butyl 3-(2-benzoylbenzofuran-3-yl)-2-methylpropanoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of butyl 3-(2-benzoylbenzofuran-3-yl)-2-methylpropanoate

There total 2 articles about butyl 3-(2-benzoylbenzofuran-3-yl)-2-methylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

2-benzoylbenzofuran (6272-40-8) + 2-methyl-butyl acrylate (97-88-1,9003-63-8) → butyl 3-(2-benzoylbenzofuran-3-yl)-2-methylpropanoate (1638610-40-8)

Guidance literature:

With tris(triphenylphosphine)ruthenium(II) chloride; silver(I) acetate; potassium carbonate; In toluene; at 140 ℃; for 12h; regioselective reaction; Inert atmosphere; Sealed tube;

DOI:10.1002/chem.201400401

Reference yield: 86.0%

→ butyl 3-(2-benzoylbenzofuran-3-yl)-2-methylpropanoate (1638610-40-8)

Guidance literature:

With tris(triphenylphosphine)ruthenium(II) chloride; silver(I) acetate; potassium carbonate; In toluene; at 140 ℃; for 24h; Inert atmosphere;

upstream raw materials:

2-benzoylbenzofuran

2-methyl-butyl acrylate

Refernces

• 1、 Kommagalla, Yadagiri,Srinivas, Kolluru,Ramana, Chepuri V.. "Ru-catalyzed branched versus linear selective C3-alkylation of 2-aroylbenzofurans with acrylates via C-H activation". supporting information. p. 7884 - 7889. Retrieved 2014/07/07.