2-octyloxybenzoic acid hydrazide

Base Information

• Chemical Name: 2-octyloxybenzoic acid hydrazide
• CAS No.: 255062-86-3
• Molecular Formula: C₁₅H₂₄N₂O₂
• Molecular Weight: 264.368
• Mol file: 255062-86-3.mol

Synonyms:2-octyloxybenzoic acid hydrazide

Chemical Property of 2-octyloxybenzoic acid hydrazide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 2-octyloxybenzoic acid hydrazide

There total 2 articles about 2-octyloxybenzoic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2-octyloxybenzoic acid methyl ester (255062-85-2) → 2-octyloxybenzoic acid hydrazide (255062-86-3)

Guidance literature:

With hydrazine hydrate; In methanol; for 12h; Heating;

DOI:10.1021/ja037312x

Reference yield:

→ 2-octyloxybenzoic acid hydrazide (255062-86-3)

Guidance literature:

Aethylester d. entsprech. substit. Benzoesaeure, Hydrazinhydrat;

Reference yield: 99.0%

2-octyloxybenzoic acid hydrazide (255062-86-3) + 1,1'-carbonyldiimidazole (530-62-1) → C16H22N2O3 (1235559-15-5)

Guidance literature:

In dichloromethane; at 20 ℃; for 3h;

DOI:10.1021/ol101068n

upstream raw materials:

2-octyloxybenzoic acid methyl ester

Downstream raw materials:

2-methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoic acid methyl ester

C₂₀H₃₀N₂O₅

C₁₈H₂₆N₂O₅

C₄₇H₇₂N₆O₁₁

Refernces

• 1、 Du, Ping,Wang, Gui-Tao,Zhao, Xin,Li, Guang-Yu,Jiang, Xi-Kui,Li, Zhan-Ting. "Two novel quadruple hydrogen-bonding motifs: the formation of supramolecular polymers, vesicles, and organogels". supporting information; experimental part. p. 188 - 191. Retrieved 2010/03/04.