Technology Process of (2,2'-bipyridine)(phenylacetylene)copper(I) hexafluoroantimonate
There total 1 articles about (2,2'-bipyridine)(phenylacetylene)copper(I) hexafluoroantimonate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
acetone;
addn. of a soln. of bpy in acetone to a soln. of Cu(NCCH3)4SbF6 in acetone under N2, addn. of phenylacetylene via a syringe to the deep red soln., stirring (1.5 h), filtration; redn. in vol. (vac.), addn. of hexane, pptn., filtration, washing (hexane, 3 times), drying (vac., overnight); elem. anal.;
DOI:10.1021/om00037a019
- Guidance literature:
-
In
acetone;
dissolving of (Cu(bpy)(HCCPh))SbF6 in acetone; addn. of hexane, pptn., filtration, two addnl. repptn., washing (hexane, 3 times), drying (vac., overnight); elem. anal.;
DOI:10.1021/om00037a019