Technology Process of 3β-{2-[4-(4-methoxybenzoyloxy)methyl-1H-1,2,3-triazol-1-yl]acetoxy}olean-12-en-28-oic acid
There total 6 articles about 3β-{2-[4-(4-methoxybenzoyloxy)methyl-1H-1,2,3-triazol-1-yl]acetoxy}olean-12-en-28-oic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
tetrahydrofuran;
at 20 ℃;
for 12h;
DOI:10.1111/cbdd.12241
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / 1,2-dimethoxyethane / 100 °C
2: dmap; potassium carbonate / dichloromethane / 0 - 20 °C
3: sodium azide / 1,2-dimethoxyethane / 75 °C
4: copper(ll) sulfate pentahydrate; sodium L-ascorbate / dichloromethane; water / 20 °C
5: hydrogen; palladium 10% on activated carbon / tetrahydrofuran / 12 h / 20 °C
With
dmap; sodium azide; copper(ll) sulfate pentahydrate; palladium 10% on activated carbon; hydrogen; potassium carbonate; sodium L-ascorbate;
In
tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water;
DOI:10.1111/cbdd.12241
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dmap; potassium carbonate / dichloromethane / 0 - 20 °C
2: sodium azide / 1,2-dimethoxyethane / 75 °C
3: copper(ll) sulfate pentahydrate; sodium L-ascorbate / dichloromethane; water / 20 °C
4: hydrogen; palladium 10% on activated carbon / tetrahydrofuran / 12 h / 20 °C
With
dmap; sodium azide; copper(ll) sulfate pentahydrate; palladium 10% on activated carbon; hydrogen; potassium carbonate; sodium L-ascorbate;
In
tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water;
DOI:10.1111/cbdd.12241