phenanthro[9,10-c][1,2, 5]thiadiazole-2,2-dioxide

Base Information

• Chemical Name: phenanthro[9,10-c][1,2, 5]thiadiazole-2,2-dioxide
• CAS No.: 4475-63-2
• Molecular Formula: C₁₄H₈N₂O₂S
• Molecular Weight: 268.296
• Mol file: 4475-63-2.mol

Synonyms:phenanthro[9,10-c][1,2, 5]thiadiazole-2,2-dioxide

Chemical Property of phenanthro[9,10-c][1,2, 5]thiadiazole-2,2-dioxide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of phenanthro[9,10-c][1,2, 5]thiadiazole-2,2-dioxide

There total 1 articles about phenanthro[9,10-c][1,2, 5]thiadiazole-2,2-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2,2-dioxo-2,3-dihydro-2λ6-thia-1,3-diaza-cyclopenta[l]phenanthren-3a-yl)-diethyl-amine → diethylamine (109-89-7) + phenanthro[9,10-c][1,2, 5]thiadiazole-2,2-dioxide (4475-63-2)

Guidance literature:

In N,N-dimethyl-formamide; Equilibrium constant;

DOI:10.1002/poc.1022

Reference yield: 97.0%

1,2-diamino-benzene (95-54-5) + phenanthro[9,10-c][1,2, 5]thiadiazole-2,2-dioxide (4475-63-2) → dibenzo[a,c]phenacine (215-64-5)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

DOI:10.1002/poc.1444

Reference yield:

ethylenediamine (107-15-3,85404-18-8) + phenanthro[9,10-c][1,2, 5]thiadiazole-2,2-dioxide (4475-63-2) → dibenzo[f,h]quinoxaline (217-68-5)

Guidance literature:

In chloroform-d1; at 20 ℃; Inert atmosphere;

DOI:10.1002/poc.1444

Downstream raw materials:

dibenzo[f,h]quinoxaline

dibenzo[a,c]phenacine

Refernces