Technology Process of phenyl 4-amino-2,5-bis(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate
There total 5 articles about phenyl 4-amino-2,5-bis(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
ethyl acetate;
at 40 ℃;
for 40h;
under 30003 Torr;
DOI:10.1021/ma4010023
- Guidance literature:
-
Multi-step reaction with 3 steps
1: oxalyl dichloride / 0 - 20 °C
2: triethylamine / dichloromethane / 0 - 20 °C
3: palladium 10% on activated carbon; hydrogen / ethyl acetate / 40 h / 40 °C / 30003 Torr
With
oxalyl dichloride; palladium 10% on activated carbon; hydrogen; triethylamine;
In
dichloromethane; ethyl acetate;
DOI:10.1021/ma4010023
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: dipotassium peroxodisulfate; potassium hydroxide; water / 168 h / 20 °C
2.1: sulfuric acid / Reflux
3.1: potassium carbonate / acetone / Inert atmosphere; Reflux
3.2: 2 h / Reflux
4.1: oxalyl dichloride / 0 - 20 °C
5.1: triethylamine / dichloromethane / 0 - 20 °C
6.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 40 h / 40 °C / 30003 Torr
With
dipotassium peroxodisulfate; oxalyl dichloride; sulfuric acid; palladium 10% on activated carbon; water; hydrogen; potassium carbonate; triethylamine; potassium hydroxide;
In
dichloromethane; ethyl acetate; acetone;
1.1: |Elbs Oxidation;
DOI:10.1021/ma4010023
