Technology Process of 4-allyloxy-1-benzyl-1H-pyrazole
There total 4 articles about 4-allyloxy-1-benzyl-1H-pyrazole which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: isopropylmagnesium chloride / diethyl ether; tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
1.2: 1 h / 20 °C
2.1: dihydrogen peroxide; 2-trifluoro-methanesulfonyl-phenylselenic acid / water; dichloromethane / 24 h / 20 °C
3.1: sodium hydroxide / water; dichloromethane / 1.5 h / 50 °C
4.1: sodium hydroxide / water / 2 h / 20 °C
With
2-trifluoro-methanesulfonyl-phenylselenic acid; dihydrogen peroxide; isopropylmagnesium chloride; sodium hydroxide;
In
tetrahydrofuran; diethyl ether; dichloromethane; water;
2.1: |Baeyer-Villiger Ketone Oxidation;
DOI:10.1248/cpb.c12-00725
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydroxide / water; dichloromethane / 1.5 h / 50 °C
2: sodium hydroxide / water / 2 h / 20 °C
With
sodium hydroxide;
In
dichloromethane; water;
DOI:10.1248/cpb.c12-00725
