Technology Process of 1-(3-benzyloxy-4-methoxyphenyl)ethane-1,2-diol
There total 7 articles about 1-(3-benzyloxy-4-methoxyphenyl)ethane-1,2-diol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran; diethyl ether;
for 2h;
Inert atmosphere;
Reflux;
DOI:10.1016/j.bmc.2017.01.050
- Guidance literature:
-
With
potassium osmate; potassium carbonate; potassium hexacyanoferrate(III);
In
tert-butyl alcohol;
for 65h;
Ambient temperature;
DOI:10.1080/00397919808004875
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) potassium tert-butoxide / 1.) THF, room temperature, 1 h, 2.) THF, room temperature, 24 h
2: 89 percent / K2CO3 / acetone / 48 h / Heating
3: 70 percent / aq. K2Os2(OH)4, K3Fe(CN)6, K2CO3 / 2-methyl-propan-2-ol / 65 h / Ambient temperature
With
potassium osmate; potassium tert-butylate; potassium carbonate; potassium hexacyanoferrate(III);
In
acetone; tert-butyl alcohol;
DOI:10.1080/00397919808004875
