Technology Process of methyl 30-hydroxytriacontanoate
There total 11 articles about methyl 30-hydroxytriacontanoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
methanol;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: Mg / tetrahydrofuran
1.2: 95 percent / MeMgCl; Li2CuCl4 / tetrahydrofuran / 16 h / -20 - 20 °C
2.1: 77 percent / pyridinium chlorochromate / CH2Cl2 / 2.5 h / 20 °C
3.1: (Me3Si)2NNa / tetrahydrofuran / 1.5 h
3.2: tetrahydrofuran / 16 h / -20 - 20 °C
4.1: 42.86 g / diethyl ether
5.1: H2 / 10 percent Pd/C / ethyl acetate
6.1: TsOH / methanol / 20 °C
With
hydrogen; sodium hexamethyldisilazane; toluene-4-sulfonic acid; magnesium; pyridinium chlorochromate;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; ethyl acetate;
3.2: Wittig reaction;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: 36 percent / aq. HBr / 22 h / 80 °C
2.1: 96 percent / conc. HCl / 2.5 h / 20 °C
3.1: Mg / tetrahydrofuran
3.2: 95 percent / MeMgCl; Li2CuCl4 / tetrahydrofuran / 16 h / -20 - 20 °C
4.1: 77 percent / pyridinium chlorochromate / CH2Cl2 / 2.5 h / 20 °C
5.1: (Me3Si)2NNa / tetrahydrofuran / 1.5 h
5.2: tetrahydrofuran / 16 h / -20 - 20 °C
6.1: 42.86 g / diethyl ether
7.1: H2 / 10 percent Pd/C / ethyl acetate
8.1: TsOH / methanol / 20 °C
With
hydrogenchloride; hydrogen bromide; hydrogen; sodium hexamethyldisilazane; toluene-4-sulfonic acid; magnesium; pyridinium chlorochromate;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; ethyl acetate;
5.2: Wittig reaction;
