Technology Process of C51H59N3O3
There total 12 articles about C51H59N3O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
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Multi-step reaction with 4 steps
1: 95 percent / TBAF / tetrahydrofuran
2: 94 percent / Dess-Martin periodinane; NaHCO3 / CH2Cl2
3: 97 percent / BuLi / tetrahydrofuran
4: 90 percent / NaH / dimethylformamide
With
n-butyllithium; tetrabutyl ammonium fluoride; sodium hydride; sodium hydrogencarbonate; Dess-Martin periodane;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.05.161
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 90 percent / BH3*SMe2; BF3*OEt2 / CH2Cl2
2: 96 percent / pyridine
3: 88 percent / pyridine
4: 94 percent / NaN3 / dimethylformamide
5: 95 percent / TBAF / tetrahydrofuran
6: 94 percent / Dess-Martin periodinane; NaHCO3 / CH2Cl2
7: 97 percent / BuLi / tetrahydrofuran
8: 90 percent / NaH / dimethylformamide
With
n-butyllithium; sodium azide; dimethylsulfide borane complex; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; sodium hydride; sodium hydrogencarbonate; Dess-Martin periodane;
In
tetrahydrofuran; pyridine; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.05.161