(CH₃)2BOC(CH₃)2C(CH₃)2OH

Base Information

• Chemical Name: (CH₃)2BOC(CH₃)2C(CH₃)2OH
• CAS No.: 97782-68-8
• Molecular Formula: C₈H₁₉BO₂
• Molecular Weight: 158.049
• Mol file: 97782-68-8.mol

Synonyms:(CH₃)2BOC(CH₃)2C(CH₃)2OH

Chemical Property of (CH₃)2BOC(CH₃)2C(CH₃)2OH

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (CH₃)2BOC(CH₃)2C(CH₃)2OH

There total 1 articles about (CH₃)2BOC(CH₃)2C(CH₃)2OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

methyllithium (917-54-4) + 2,4,4,5,5-pentamethyl-[1,3,2]dioxaborolane (94242-85-0) → (CH3)2BOC(CH3)2C(CH3)2OH (97782-68-8) + trimethylborane (593-90-8)

Guidance literature:

With hydrogenchloride; In diethyl ether; byproducts: LiCl; 1 equiv of MeLi slowly adding to a soln. of the boronic ester at -78°C, stirring for 3 h at the same temp., 1 equiv of anhydrous HCl in Et2O adding, warming to room temp., stirring for 15 min; the content was detd. by (11)B NMR spectrum;

DOI:10.1021/om00129a019

upstream raw materials:

methyllithium

2,4,4,5,5-pentamethyl-[1,3,2]dioxaborolane

Refernces