Mo₄O₂I₂(O-i-Pr)6

Base Information

• Chemical Name: Mo₄O₂I₂(O-i-Pr)6
• CAS No.: 113810-70-1
• Molecular Formula: C₁₈H₄₂I₂Mo₄O₈
• Molecular Weight: 1024.1
• Mol file: 113810-70-1.mol

Synonyms:Mo₄O₂I₂(O-i-Pr)6

Chemical Property of Mo₄O₂I₂(O-i-Pr)6

Chemical Property:

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Technology Process of Mo₄O₂I₂(O-i-Pr)6

There total 1 articles about Mo₄O₂I₂(O-i-Pr)6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Mo2(O-i-Pr)6 (62521-20-4) + trimethylsilyl iodide (16029-98-4) → 2-iodo-propane (75-30-9) + Mo4O2I2(O-i-Pr)6 (113810-70-1) + isopropoxytrimethylsilane (1825-64-5)

Guidance literature:

In toluene; Mo2(O-i-Pr)6 was dissolved in toluene uner N2, and the mixt. was cooled to -78°C. Iodotrimethylsilane was added dropwise. The soln. was allowed to warm to room temp.. After 3 h at room temp. the mixt. was warmed to 55°C and stirred (2 d).; The soln. was reduced in vol. by half and cooled to -15°C. After 2 d a ppt. was isolated by filtration and dried in vacuo.;

upstream raw materials:

Mo₂(O-i-Pr)6

trimethylsilyl iodide

Refernces