1-phenacyl-2,5-dihydrothiophenium bromide

Base Information Edit

Chemical Name:1-phenacyl-2,5-dihydrothiophenium bromide
CAS No.:69520-31-6
Molecular Formula:Br*C₁₂H₁₃OS
Molecular Weight:285.205
Hs Code.:
Mol file:69520-31-6.mol

Synonyms:1-phenacyl-2,5-dihydrothiophenium bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phenacyl-2,5-dihydrothiophenium bromide Edit

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Technology Process of 1-phenacyl-2,5-dihydrothiophenium bromide

There total 1 articles about 1-phenacyl-2,5-dihydrothiophenium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1708-32-3
2,5-dihydro-thiophene

: 70-11-1
α-bromoacetophenone

: 69520-31-6
1-phenacyl-2,5-dihydrothiophenium bromide

Guidance literature:: In acetonitrile;
DOI:10.1039/P19810001953

Reference yield:

: 69520-31-6
1-phenacyl-2,5-dihydrothiophenium bromide

: 98-85-1,13323-81-4
1-Phenylethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 680 mg / 22percent sodium hydroxide / H₂O

2: 300 mg / benzene / 1 h / Heating

3: 300 mg / Raney nickel / methanol / 15 h / Heating

With sodium hydroxide; nickel; In methanol; water; benzene;
DOI:10.1039/P19810001953