Technology Process of 5-methyl-1-nitroso-2-phenylindoline
There total 5 articles about 5-methyl-1-nitroso-2-phenylindoline which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride; sodium nitrite;
In
water;
at 0 - 20 ℃;
for 1.08333h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sulfuric acid / 1,4-dioxane / 6 h / 100 °C
2.1: phosphoric acid / 2 h / 100 °C
2.2: 20 °C
3.1: sodium cyanoborohydride; acetic acid / 4 h / 20 °C
4.1: hydrogenchloride; sodium nitrite / water / 1.08 h / 0 - 20 °C
With
hydrogenchloride; phosphoric acid; sulfuric acid; sodium cyanoborohydride; acetic acid; sodium nitrite;
In
1,4-dioxane; water;
1.1: Fischer Indole Synthesis;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium cyanoborohydride; acetic acid / 4 h / 20 °C
2: hydrogenchloride; sodium nitrite / water / 1.08 h / 0 - 20 °C
With
hydrogenchloride; sodium cyanoborohydride; acetic acid; sodium nitrite;
In
water;
