mesityl-glyoxal-2-hydrazone

Base Information

• Chemical Name: mesityl-glyoxal-2-hydrazone
• CAS No.: 23722-23-8
• Molecular Formula: C₁₁H₁₄N₂O
• Molecular Weight: 190.245
• Mol file: 23722-23-8.mol

Synonyms:mesityl-glyoxal-2-hydrazone

Chemical Property of mesityl-glyoxal-2-hydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of mesityl-glyoxal-2-hydrazone

There total 2 articles about mesityl-glyoxal-2-hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

mesitylglyoxal (22185-97-3) + hydrazinium monoacetate (7335-65-1,13255-48-6) → mesityl-glyoxal-2-hydrazone (23722-23-8)

Guidance literature:

With ethanol;

DOI:10.1021/ja01234a037

Reference yield:

2-bromo-1-(2,4,6-trimethylphenyl)ethanone (4225-92-7) → mesityl-glyoxal-2-hydrazone (23722-23-8)

Guidance literature:

With hydrazine hydrate;

Reference yield:

mesityl-glyoxal-2-hydrazone (23722-23-8) → 2-diazo-1-mesityl-ethanone (13661-19-3)

Guidance literature:

With calcium sulfate; mercury(II) oxide; Petroleum ether; weiteres Reagens: aethanol. KOH;

DOI:10.1021/ja01234a037

upstream raw materials:

mesitylglyoxal

hydrazinium monoacetate

2-bromo-1-(2,4,6-trimethylphenyl)ethanone

Downstream raw materials:

2-diazo-1-mesityl-ethanone