Technology Process of 4,4'-[Octane-1,6-diylbis(oxy)]dianiline
There total 8 articles about 4,4'-[Octane-1,6-diylbis(oxy)]dianiline which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrazine hydrate;
In
ethanol;
for 3h;
Reflux;
DOI:10.1039/c4ra06211f
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 6 h / 50 °C
1.2: 0 - 30 °C
2.1: palladium 10% on activated carbon; hydrazine hydrate / ethanol / 3 h / Reflux
With
palladium 10% on activated carbon; sodium hydride; hydrazine hydrate;
In
ethanol; N,N-dimethyl-formamide;
DOI:10.1039/c4ra06211f
- Guidance literature:
-
With
sodium hydrogencarbonate;
In
water;
for 1h;