2,6-Dichlorophenyl chloroformate

Base Information

• Chemical Name: 2,6-Dichlorophenyl chloroformate
• CAS No.: 374568-08-8
• Molecular Formula: C₇H₃Cl₃O₂
• Molecular Weight: 225.459
• Mol file: 374568-08-8.mol

Synonyms:2,6-Dichlorophenyl chloroformate

Chemical Property of 2,6-Dichlorophenyl chloroformate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,6-Dichlorophenyl chloroformate

There total 1 articles about 2,6-Dichlorophenyl chloroformate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

phosgene (75-44-5) + 2,6-Dichlorophenol (87-65-0) → 2,6-Dichlorophenyl chloroformate (374568-08-8)

Guidance literature:

With N,N-dimethyl-aniline; In toluene; Inert atmosphere;

DOI:10.1016/j.tetlet.2008.08.081

Reference yield: 92.0%

C63H60N3O6P3*3ClH + 2,6-Dichlorophenyl chloroformate (374568-08-8) → C30H21Cl6N3O12 (1083072-44-9)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; Inert atmosphere; Cooling with ice;

DOI:10.1016/j.tetlet.2008.08.081

Reference yield:

2-amino-1,2,3,4-tetrahydro-isoquinoline-hydrochloride (79492-26-5) + 2,6-Dichlorophenyl chloroformate (374568-08-8) → (3,4-Dihydro-1H-isoquinolin-2-yl)-carbamic Acid 2.6-dichloro-phenyl Ester

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane;

upstream raw materials:

phosgene

2,6-Dichlorophenol

Downstream raw materials:

C₃₀H₂₁Cl₆N₃O₁₂

Refernces