(S)-(Z)-[2-(5-hydroxy-2-methylene-cyclohexylidene)ethyl]di-phenylphosphineoxide

Base Information Edit

Chemical Name:(S)-(Z)-[2-(5-hydroxy-2-methylene-cyclohexylidene)ethyl]di-phenylphosphineoxide
CAS No.:1236132-10-7
Molecular Formula:C₂₁H₂₃O₂P
Molecular Weight:338.386
Hs Code.:
Mol file:1236132-10-7.mol

Synonyms:(S)-(Z)-[2-(5-hydroxy-2-methylene-cyclohexylidene)ethyl]di-phenylphosphineoxide

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Chemical Property of (S)-(Z)-[2-(5-hydroxy-2-methylene-cyclohexylidene)ethyl]di-phenylphosphineoxide Edit

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Technology Process of (S)-(Z)-[2-(5-hydroxy-2-methylene-cyclohexylidene)ethyl]di-phenylphosphineoxide

There total 5 articles about (S)-(Z)-[2-(5-hydroxy-2-methylene-cyclohexylidene)ethyl]di-phenylphosphineoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 100858-27-3
(S)-(Z)-{2-[5-(tert-butyldimethylsiloxy)-2-methylenecyclohexylidene]ethyl}diphenylphosphine oxide

: 1236132-10-7
(S)-(Z)-[2-(5-hydroxy-2-methylene-cyclohexylidene)ethyl]di-phenylphosphineoxide

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 5h;
DOI:10.1016/j.tet.2010.04.051

Reference yield:

: 66251-15-8
Benzoic acid (S)-3-[2-hydroxy-eth-(Z)-ylidene]-4-methylene-cyclohexyl ester

: 1236132-10-7
(S)-(Z)-[2-(5-hydroxy-2-methylene-cyclohexylidene)ethyl]di-phenylphosphineoxide

Guidance literature:: Multi-step reaction with 3 steps

1: chloromethylene-dimethyl-ammonium chloride / dimethylformamide

2: tetrahydrofuran

3: aq. NaOH, MeOH

With methanol; sodium hydroxide; Vilsmeier reagent; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 68323-44-4
Benzoic acid (S)-3-[2-chloro-eth-(Z)-ylidene]-4-methylene-cyclohexyl ester

: 1236132-10-7
(S)-(Z)-[2-(5-hydroxy-2-methylene-cyclohexylidene)ethyl]di-phenylphosphineoxide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: aq. NaOH, MeOH

With methanol; sodium hydroxide; In tetrahydrofuran;