(Z)-α-Phenyl-β-nitro-4-nitrocinnamonitril

Base Information

• Chemical Name: (Z)-α-Phenyl-β-nitro-4-nitrocinnamonitril
• CAS No.: 72433-39-7
• Molecular Formula: C₁₅H₉N₃O₄
• Molecular Weight: 295.254
• Mol file: 72433-39-7.mol

Synonyms:(Z)-α-Phenyl-β-nitro-4-nitrocinnamonitril

Chemical Property of (Z)-α-Phenyl-β-nitro-4-nitrocinnamonitril

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Z)-α-Phenyl-β-nitro-4-nitrocinnamonitril

There total 2 articles about (Z)-α-Phenyl-β-nitro-4-nitrocinnamonitril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

(2Z)-2-(phenyl)-3-(4’-nitrophenyl)acrylonitrile (7431-35-8,10077-28-8,62297-44-3) → (Z)-α-Phenyl-β-nitro-4-nitrocinnamonitril (72433-39-7)

Guidance literature:

With mixed nitrogen oxides; iodine; In tetrachloromethane; at -5 ℃; for 3h;

DOI:10.1080/00304949909355681

Reference yield:

4-nitrobenzaldehdye (555-16-8) → (Z)-α-Phenyl-β-nitro-4-nitrocinnamonitril (72433-39-7)

Guidance literature:

Multi-step reaction with 2 steps

2: N₂O₄ / CCl₄

With dinitrogen tetraoxide; In tetrachloromethane;

Reference yield:

(Z)-α-Phenyl-β-nitro-4-nitrocinnamonitril (72433-39-7) → p-nitrodeoxybenzoin (3769-84-4)

Guidance literature:

With hydrogenchloride; iron; In ethanol; Heating;

upstream raw materials:

(2Z)-2-(phenyl)-3-(4’-nitrophenyl)acrylonitrile

4-nitrobenzaldehdye

Downstream raw materials:

p-nitrodeoxybenzoin

β-Amino-β-4-nitrophenyl-α-phenylacrylamid

Refernces