2,6-Dichlor-p-benzochinonmonoimin

Base Information

• Chemical Name: 2,6-Dichlor-p-benzochinonmonoimin
• CAS No.: 2852-70-2
• Molecular Formula: C₆H₃Cl₂NO
• Molecular Weight: 176.002
• Mol file: 2852-70-2.mol

Synonyms:2,6-Dichlor-p-benzochinonmonoimin

Chemical Property of 2,6-Dichlor-p-benzochinonmonoimin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,6-Dichlor-p-benzochinonmonoimin

There total 3 articles about 2,6-Dichlor-p-benzochinonmonoimin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,6-dichloroquinone-4-chloroimide (101-38-2) + ethanol (64-17-5) → 2,6-Dichlor-p-benzochinonmonoimin (2852-70-2) + acetaldehyde (75-07-0,9002-91-9)

Guidance literature:

With N-butylamine; In acetonitrile; at 34.9 ℃; Kinetics; Thermodynamic data; temperature dependence of the rate constants, in the presence of various amines, and various polarity of the solvent; ΔH(excit.), ΔS(excit.), ΔG(excit.);

DOI:10.1039/P29860000105

Reference yield:

2,6-dichloroquinone-4-chloroimide (101-38-2) + 4-amino-2,6-dichlorophenol (5930-28-9) → 2,6-Dichlor-p-benzochinonmonoimin (2852-70-2)

Guidance literature:

With ascorbic acid; In water; acetone;

DOI:10.1039/P29860000105

Reference yield:

2,6-dichloroquinone-4-chloroimide (101-38-2) → 2,6-Dichlor-p-benzochinonmonoimin (2852-70-2)

Guidance literature:

With p-benzoquinone; In [D₃]acetonitrile; water-d2; pH=9.2; Further Variations:; Reagents; Product distribution;

DOI:10.1021/jo982113v

upstream raw materials:

2,6-dichloroquinone-4-chloroimide

ethanol

4-amino-2,6-dichlorophenol

Refernces

• 1、 Pallagi, Istvan,Dvortsak, Peter. "GIBBS REACTION. PART 1. REDUCTION OF BENZOQUINONE N-CHLOROIMINES TO BENZOQUINONE IMINES". . p. 105 - 110. Retrieved 1986.