Technology Process of 2,4,5-trichloro-benzoic acid amide
There total 12 articles about 2,4,5-trichloro-benzoic acid amide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
thionyl chloride; ammonia;
Yield given. Multistep reaction;
1) reflux, 2) benzene;
DOI:10.1021/jo00001a022
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1) 30percent Oleum, 2) ice / 1) 100 deg C, 24 h
2: 1) SOCl2, 2) ammonia / 1) reflux, 2) benzene
With
thionyl chloride; sulfuric acid; Methamphetamin; ammonia;
DOI:10.1021/jo00001a022
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 77 percent / 1a) AlCl3, 1b) AlCl3 / 1a) 8 h, r.t., 1b) 16 h, -10 deg C
2: 1) 30percent Oleum, 2) ice / 1) 100 deg C, 24 h
3: 1) SOCl2, 2) ammonia / 1) reflux, 2) benzene
With
aluminium trichloride; thionyl chloride; sulfuric acid; Methamphetamin; ammonia;
DOI:10.1021/jo00001a022
