2,2'-(Ethane-1,2-diyldisulfonyl)diethanol

Base Information

• Chemical Name: 2,2'-(Ethane-1,2-diyldisulfonyl)diethanol
• CAS No.: 7484-34-6
• Molecular Formula: C₆H₁₄O₆S₂
• Molecular Weight: 246.306
• NSC Number: 191911
• DSSTox Substance ID: DTXSID30307519
• Nikkaji Number: J25.787G
• Wikidata: Q82054934
• Mol file: 7484-34-6.mol

Synonyms:2,2'-(Ethane-1,2-diyldisulfonyl)diethanol;7484-34-6;2-[2-(2-hydroxyethylsulfonyl)ethylsulfonyl]ethanol;2,2'-(Ethylenebissulfonyl)diethanol;NSC191911;DTXSID30307519;MFCD27923650;AKOS022178234;DS-3087;NSC-191911;CS-0158307;Ethanol, 2,2'-(1,2-ethanediyldisulfonyl)bis-;A865792;2,2'-(ethane-1,2-diyldisulfonyl)bis(ethan-1-ol);2-[2-(2-hydroxyethanesulfonyl)ethanesulfonyl]ethan-1-ol

Chemical Property of 2,2'-(Ethane-1,2-diyldisulfonyl)diethanol

Chemical Property:

• Boiling Point: 627.9oC at 760 mmHg
• Flash Point: 333.5oC
• PSA: 125.50000
• Density: 1.495g/cm3
• LogP: -0.03780
• Storage Temp.: 2-8°C
• XLogP3: -2.4
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 7
• Exact Mass: 246.02318051
• Heavy Atom Count: 14
• Complexity: 294

Purity/Quality:

99% ^*data from raw suppliers

2,2'-(Ethane-1,2-diyldisulfonyl)diethanol >95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(CS(=O)(=O)CCS(=O)(=O)CCO)O

Technology Process of 2,2'-(Ethane-1,2-diyldisulfonyl)diethanol

There total 2 articles about 2,2'-(Ethane-1,2-diyldisulfonyl)diethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2,2'-ethane-1,2-diylbissulfanyl-bis-ethanol (5244-34-8) → 1,2-bis(2-hydroxyethylsulfonyl)ethane (7484-34-6)

Guidance literature:

With Oxone; In neat (no solvent); for 1.5h; chemoselective reaction; Milling; Green chemistry;

DOI:10.1039/c2cc36365h

Reference yield:

→ 1,2-bis(2-hydroxyethylsulfonyl)ethane (7484-34-6)

Guidance literature:

entspr. Disulfid, H2O2;

Reference yield:

1,2-bis(2-hydroxyethylsulfonyl)ethane (7484-34-6) + benzoyl chloride (98-88-4) → 1,2-bis-(2-benzoyloxy-ethanesulfonyl)-ethane

Guidance literature:

DOI:10.1021/jo01166a008

upstream raw materials:

2,2'-ethane-1,2-diylbissulfanyl-bis-ethanol

Refernces

• 1、 Timperley, Christopher M.,Black, Robin M.,Bird, Michael,Holden, Ian,Mundy, Joanna L.,Read, Robert W.. "Hydrolysis and oxidation products of the chemical warfare agents 1,2-Bis[(2-chloroethyl)thio]ethane Q and 2,2′-Bis(2-chloroethylthio) diethyl ether T". . p. 2027 - 2046. Retrieved 2007/10/03.