C₂₅H₂₈N₂O₃S

Base Information Edit

Chemical Name:C₂₅H₂₈N₂O₃S
CAS No.:1451192-90-7
Molecular Formula:C₂₅H₂₈N₂O₃S
Molecular Weight:436.575
Hs Code.:
Mol file:1451192-90-7.mol

C<sub>25</sub>H<sub>28</sub>N<sub>2</sub>O<sub>3</sub>S

Synonyms:C₂₅H₂₈N₂O₃S

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Chemical Property of C₂₅H₂₈N₂O₃S Edit

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Technology Process of C₂₅H₂₈N₂O₃S

There total 14 articles about C₂₅H₂₈N₂O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1451192-94-1
C₂₃H₂₄N₂O₂S

: 540-51-2
2-bromoethanol

: 1451192-90-7
C₂₅H₂₈N₂O₃S

Guidance literature:: With sodium carbonate; In ethanol; at 85 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ja408114u

Reference yield:

: 1451192-86-1
C₂₉H₃₆N₂O₅S₂

: 1451192-90-7
C₂₅H₂₈N₂O₃S

Guidance literature:: Multi-step reaction with 6 steps

1.1: diisobutylaluminium hydride / dichloromethane / 1 h / 0 °C / Inert atmosphere

2.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.67 h / -78 - 0 °C / Inert atmosphere

3.2: 2 h / -78 - 20 °C / Inert atmosphere

4.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 48 h / 20 °C / Inert atmosphere

5.1: hydrogenchloride / methanol; water / 0 °C / Inert atmosphere

6.1: sodium carbonate / ethanol / 24 h / 85 °C / Inert atmosphere

With hydrogenchloride; n-butyllithium; Hoveyda-Grubbs catalyst second generation; diisobutylaluminium hydride; sodium hydrogencarbonate; sodium carbonate; Dess-Martin periodane; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water;
DOI:10.1021/ja408114u

Reference yield:

: 1451192-88-3
C₂₈H₃₄N₂O₄S₂

: 1451192-90-7
C₂₅H₂₈N₂O₃S

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.67 h / -78 - 0 °C / Inert atmosphere

1.2: 2 h / -78 - 20 °C / Inert atmosphere

2.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 48 h / 20 °C / Inert atmosphere

3.1: hydrogenchloride / methanol; water / 0 °C / Inert atmosphere

4.1: sodium carbonate / ethanol / 24 h / 85 °C / Inert atmosphere

With hydrogenchloride; n-butyllithium; Hoveyda-Grubbs catalyst second generation; sodium carbonate; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water;
DOI:10.1021/ja408114u