(25R)-5alpha-Spirostan-3beta-yl acetate

Base Information Edit

Chemical Name:(25R)-5alpha-Spirostan-3beta-yl acetate
CAS No.:2530-07-6
Molecular Formula:C29H46O4
Molecular Weight:458.682
Hs Code.:
European Community (EC) Number:219-777-4
DSSTox Substance ID:DTXSID60948136
Nikkaji Number:J82.440B
Wikidata:Q82925924
Mol file:2530-07-6.mol

Synonyms:2530-07-6;Tigogenin acetate;(25R)-5alpha-Spirostan-3beta-yl acetate;[(1R,2S,4S,5'R,6R,7S,8R,9S,12S,13S,16S,18S)-5',7,9,13-tetramethylspiro[5-oxapentacyclo[10.8.0.02,9.04,8.013,18]icosane-6,2'-oxane]-16-yl] acetate;Acetyltigogenin;SCHEMBL7996285;DTXSID60948136;EINECS 219-777-4;(1'R,2R,2'S,4'S,5R,7'S,8'R,9'S,12'S,13'S,16'S,18'S)-5,7',9',13'-tetramethyl-5'-oxaspiro[oxane-2,6'-pentacyclo[10.8.0.0,.0,.0,icosan]-16'-yl acetate;(2AS,2'R,4S,5'R,6aS,6bS,8aS,8bR,9S,11aS,12aS,12bR)-5',6a,8a,9-tetramethyldocosahydrospiro[naphtho[2',1':4,5]indeno[2,1-b]furan-10,2'-pyran]-4-yl acetate

Suppliers and Price of (25R)-5alpha-Spirostan-3beta-yl acetate

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Arctom
Tigogeninacetate
10mg
$ 318.00

Total 6 raw suppliers

Chemical Property of (25R)-5alpha-Spirostan-3beta-yl acetate Edit

Chemical Property:

Vapor Pressure:3.23E-11mmHg at 25°C
Refractive Index:1.539
Boiling Point:527.5 °C at 760 mmHg
Flash Point:221.8 °C
PSA：44.76000
Density:1.11 g/cm³
LogP:6.36460
XLogP3:7.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:458.33960994
Heavy Atom Count:33
Complexity:797

Purity/Quality:

99% ^*data from raw suppliers

Tigogeninacetate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:CC1CCC2(C(C3C(O2)CC4C3(CCC5C4CCC6C5(CCC(C6)OC(=O)C)C)C)C)OC1
Isomeric SMILES:C[C@@H]1CC[C@@]2([C@H]([C@H]3[C@@H](O2)C[C@@H]4[C@@]3(CC[C@H]5[C@H]4CC[C@@H]6[C@@]5(CC[C@@H](C6)OC(=O)C)C)C)C)OC1

Technology Process of (25R)-5alpha-Spirostan-3beta-yl acetate

There total 42 articles about (25R)-5alpha-Spirostan-3beta-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 77-60-1
tigogenin

: 108-24-7
acetic anhydride

: 2530-07-6
tigogenin acetate

Guidance literature:: With pyridine; at 45 ℃;
DOI:10.1016/j.tetlet.2007.03.001

Reference yield: 92.0%

: 39636-34-5,65243-90-5,82858-54-6,107243-02-7,121349-68-6,121421-12-3
dihydrotigogenin 3-acetate

: 2530-07-6,2752-97-8,4947-75-5,4948-43-0,6870-09-3,10158-77-7,16653-26-2,35319-91-6,106759-13-1,106759-14-2,122291-16-1
tigogenin acetate

Guidance literature:: With [bis(acetoxy)iodo]benzene; iodine; In cyclohexane; at 40 ℃; for 0.666667h; Irradiation;

Reference yield: 34.0%

: 24742-79-8
(25R)-3β-Acetoxy-5α-spirostan-15-on

: 78179-65-4
(25R)-3β-acetoxy-5α-spirost-14-en

: 2530-07-6
tigogenin acetate

Guidance literature:: With toluene-4-sulfonic acid; ethane-1,2-dithiol; Urushibara-nickel; Yield given. Multistep reaction; 1) 16 h, room temp.; 2) ethanol, 2 h, reflux;