Technology Process of 2-((2,3-dimethoxybenzylidene)hydrazono)-3-methyl-2,3-dihydrobenzo[d]thiazole
There total 4 articles about 2-((2,3-dimethoxybenzylidene)hydrazono)-3-methyl-2,3-dihydrobenzo[d]thiazole which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-methylthio-3-methylbenzothiazolium iodide;
With
amino aminoalcohol;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 3h;
2,3-dimethyoxybenzaldehyde;
In
methanol; N,N-dimethyl-formamide;
for 12h;
Reflux;
DOI:10.1039/c5ra12925g
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 0 - 20 °C
2.1: 12 h / 50 - 60 °C
3.1: amino aminoalcohol / N,N-dimethyl-formamide / 3 h / 20 °C
3.2: 12 h / Reflux
With
amino aminoalcohol; potassium carbonate;
In
N,N-dimethyl-formamide;
DOI:10.1039/c5ra12925g
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 12 h / 50 - 60 °C
2.1: amino aminoalcohol / N,N-dimethyl-formamide / 3 h / 20 °C
2.2: 12 h / Reflux
With
amino aminoalcohol;
In
N,N-dimethyl-formamide;
DOI:10.1039/c5ra12925g