Technology Process of 6-ethoxy-3-phenyl-6H-dibenz[c,e][1,2]oxaphosphorin-6-oxide
There total 5 articles about 6-ethoxy-3-phenyl-6H-dibenz[c,e][1,2]oxaphosphorin-6-oxide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-Ac-Leu; [bis(acetoxy)iodo]benzene; potassium acetate; palladium diacetate;
In
tert-butyl alcohol;
at 100 ℃;
for 12h;
DOI:10.3762/bjoc.10.120
- Guidance literature:
-
Multi-step reaction with 4 steps
1: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / water; 1,2-dimethoxyethane
2: n-butyllithium / tetrahydrofuran
3: L-Selectride / tetrahydrofuran
4: palladium diacetate; N-Ac-Leu; [bis(acetoxy)iodo]benzene; potassium acetate / tert-butyl alcohol / 12 h / 100 °C
With
bis-triphenylphosphine-palladium(II) chloride; n-butyllithium; N-Ac-Leu; [bis(acetoxy)iodo]benzene; potassium acetate; palladium diacetate; L-Selectride; potassium carbonate;
In
tetrahydrofuran; 1,2-dimethoxyethane; water; tert-butyl alcohol;
1: |Suzuki Coupling;
DOI:10.3762/bjoc.10.120
- Guidance literature:
-
Multi-step reaction with 3 steps
1: n-butyllithium / tetrahydrofuran
2: L-Selectride / tetrahydrofuran
3: palladium diacetate; N-Ac-Leu; [bis(acetoxy)iodo]benzene; potassium acetate / tert-butyl alcohol / 12 h / 100 °C
With
n-butyllithium; N-Ac-Leu; [bis(acetoxy)iodo]benzene; potassium acetate; palladium diacetate; L-Selectride;
In
tetrahydrofuran; tert-butyl alcohol;
DOI:10.3762/bjoc.10.120