C₅₇H₁₀₀N₆O₁₅

Base Information

• Chemical Name: C₅₇H₁₀₀N₆O₁₅
• CAS No.: 1365682-09-2
• Molecular Formula: C₅₇H₁₀₀N₆O₁₅
• Molecular Weight: 1109.45
• Mol file: 1365682-09-2.mol

Synonyms:C₅₇H₁₀₀N₆O₁₅

Chemical Property of C₅₇H₁₀₀N₆O₁₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₇H₁₀₀N₆O₁₅

There total 12 articles about C₅₇H₁₀₀N₆O₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

C57H102N6O15 (1365681-81-7) → C57H100N6O15 (1365682-09-2)

Guidance literature:

C₅₇H₁₀₂N₆O₁₅; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.333333h; Inert atmosphere;

With triethylamine; In dichloromethane; at -78 - 20 ℃; for 6h; Inert atmosphere;

DOI:10.1021/ja2107564

Reference yield:

C15H24N2O3 → C57H100N6O15 (1365682-09-2)

Guidance literature:

Multi-step reaction with 11 steps

1.1: sodium tetrahydroborate; ethanol / 5 h / 20 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 16 h / 20 °C / Inert atmosphere

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

3.2: 6 h / -78 - 20 °C / Inert atmosphere

4.1: ethanol / 16 h / 20 °C / Inert atmosphere

5.1: sodium tetrahydroborate; ethanol / 5 h / 20 °C / Inert atmosphere

6.1: triethylamine / dichloromethane / 16 h / 20 °C / Inert atmosphere

7.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

7.2: 6 h / -78 - 20 °C / Inert atmosphere

8.1: ethanol / 16 h / 20 °C / Inert atmosphere

9.1: sodium tetrahydroborate; ethanol / 5 h / 20 °C / Inert atmosphere

10.1: triethylamine / dichloromethane / 16 h / 20 °C / Inert atmosphere

11.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

11.2: 6 h / -78 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; oxalyl dichloride; ethanol; dimethyl sulfoxide; triethylamine; In ethanol; dichloromethane; 3.1: Swern oxidation / 3.2: Swern oxidation / 7.1: Swern oxidation / 7.2: Swern oxidation / 11.1: Swern oxidation / 11.2: Swern oxidation;

DOI:10.1021/ja2107564

Reference yield:

3-(3-aminopropylamino)propan-1-ol (40226-15-1) → C57H100N6O15 (1365682-09-2)

Guidance literature:

Multi-step reaction with 12 steps

1.1: ethanol / 16 h / 20 °C / Inert atmosphere

2.1: sodium tetrahydroborate; ethanol / 5 h / 20 °C / Inert atmosphere

3.1: triethylamine / dichloromethane / 16 h / 20 °C / Inert atmosphere

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

4.2: 6 h / -78 - 20 °C / Inert atmosphere

5.1: ethanol / 16 h / 20 °C / Inert atmosphere

6.1: sodium tetrahydroborate; ethanol / 5 h / 20 °C / Inert atmosphere

7.1: triethylamine / dichloromethane / 16 h / 20 °C / Inert atmosphere

8.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

8.2: 6 h / -78 - 20 °C / Inert atmosphere

9.1: ethanol / 16 h / 20 °C / Inert atmosphere

10.1: sodium tetrahydroborate; ethanol / 5 h / 20 °C / Inert atmosphere

11.1: triethylamine / dichloromethane / 16 h / 20 °C / Inert atmosphere

12.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

12.2: 6 h / -78 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; oxalyl dichloride; ethanol; dimethyl sulfoxide; triethylamine; In ethanol; dichloromethane; 4.1: Swern oxidation / 4.2: Swern oxidation / 8.1: Swern oxidation / 8.2: Swern oxidation / 12.1: Swern oxidation / 12.2: Swern oxidation;

DOI:10.1021/ja2107564

upstream raw materials:

C₂₅H₄₀N₂O₇

C₄₁H₇₀N₄O₁₁

C₄₁H₇₂N₄O₁₁

C₅₇H₁₀₂N₆O₁₅

Refernces