C₁₇H₁₈N₂

Base Information

• Chemical Name: C₁₇H₁₈N₂
• CAS No.: 1333397-47-9
• Molecular Formula: C₁₇H₁₈N₂
• Molecular Weight: 250.343
• Mol file: 1333397-47-9.mol

Synonyms:C₁₇H₁₈N₂

Chemical Property of C₁₇H₁₈N₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₁₈N₂

There total 5 articles about C₁₇H₁₈N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C12H14N2O2 → C17H18N2 (1333397-47-9)

Guidance literature:

With sodium dithionite; sodium hydroxide; In ethanol; at 80 ℃; for 1h;

DOI:10.1055/s-0031-1290565

Reference yield:

2,3-Dimethyl-5-nitro-1H-indole (21296-94-6) → C17H18N2 (1333397-47-9)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium hydroxide / acetone / 20 °C

2: sodium dithionite; sodium hydroxide / ethanol / 1 h / 80 °C

With sodium dithionite; potassium hydroxide; sodium hydroxide; In ethanol; acetone;

DOI:10.1055/s-0031-1290565

Reference yield:

4-nitro-aniline (100-01-6,104810-17-5) → C17H18N2 (1333397-47-9)

Guidance literature:

Multi-step reaction with 5 steps

1: hydrogenchloride; sodium nitrite

2: acetic acid / ethanol

3: hydrogenchloride / 12 h / Reflux

4: potassium hydroxide / acetone / 20 °C

5: sodium dithionite; sodium hydroxide / ethanol / 1 h / 80 °C

With hydrogenchloride; sodium dithionite; acetic acid; potassium hydroxide; sodium hydroxide; sodium nitrite; In ethanol; acetone;

DOI:10.1055/s-0031-1290565

upstream raw materials:

2,3-Dimethyl-5-nitro-1H-indole

4-nitro-aniline

4-nitrophenylhydrazone

butan-2-one-(4-nitro-phenylhydrazone)

Downstream raw materials:

3-benzyl-1,2-dimethyl-3,12-dihydrochromeno[4,3-b]pyrrolo[3,2-f]quinoline

3-benzyl-1,2-dimethyl-7,9-diphenyl-3H-pyrrolo[3,2-f]quinoline

7-benzyl-8,9-dimethyl-2,4-diphenyl-7H-pyrrolo[2,3-h]quinoline

Refernces