2,4-diphenyl-9H-pyrimido[4,5-b]indole

Base Information Edit

Chemical Name:2,4-diphenyl-9H-pyrimido[4,5-b]indole
CAS No.:56807-26-2
Molecular Formula:C₂₂H₁₅N₃
Molecular Weight:321.381
Hs Code.:
Mol file:56807-26-2.mol

Synonyms:2,4-diphenyl-9H-pyrimido[4,5-b]indole

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Chemical Property of 2,4-diphenyl-9H-pyrimido[4,5-b]indole Edit

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Technology Process of 2,4-diphenyl-9H-pyrimido[4,5-b]indole

There total 9 articles about 2,4-diphenyl-9H-pyrimido[4,5-b]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: C₁₀H₅Cl₂N₃

: 98-80-6
phenylboronic acid

: 56807-26-2
2,4-diphenyl-9H-pyrimido[4,5-b]indole

Guidance literature:: With palladium diacetate; sodium carbonate; tris-(o-tolyl)phosphine; In monoethylene glycol diethyl ether; water; for 16h; Reflux;

Reference yield: 80.0%

: 100-52-7
benzaldehyde

: 139409-34-0
2-bromo-1H-indole

: 56807-26-2
2,4-diphenyl-9H-pyrimido[4,5-b]indole

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; ammonium hydroxide; copper(l) iodide; Trimethylacetic acid; In N,N-dimethyl-formamide; at 80 ℃; for 18h; Sealed tube;
DOI:10.1021/acs.joc.5b00239