C₃₇H₃₈N₂O₉

Base Information

• Chemical Name: C₃₇H₃₈N₂O₉
• CAS No.: 120268-62-4
• Molecular Formula: C₃₇H₃₈N₂O₉
• Molecular Weight: 654.717
• Mol file: 120268-62-4.mol

Synonyms:C₃₇H₃₈N₂O₉

Chemical Property of C₃₇H₃₈N₂O₉

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₇H₃₈N₂O₉

There total 6 articles about C₃₇H₃₈N₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose (6974-32-9) + 5-Hexyl-2,4-dimethoxy-pyrimidine (120268-57-7) → C37H38N2O9 (120268-62-4)

Guidance literature:

With tin(IV) chloride; In acetonitrile; Ambient temperature;

DOI:10.1248/cpb.36.2673

Reference yield:

diethyl 2-hexylmalonate (5398-10-7) → C37H38N2O9 (120268-62-4)

Guidance literature:

Multi-step reaction with 6 steps

1: sodium ethoxide / dimethylformamide

2: phosphoryl chloride, N,N-diethylaniline hydrochloride / butyl acetate / Heating

3: acetonitrile / 1 h

4: potassium tert-butoxide / 2 h / 75 °C

5: Raney Ni W-2 / ethanol / 3 h / Heating

6: 99 percent / stannic chloride / acetonitrile / Ambient temperature

With Raney Ni W-2; potassium tert-butylate; sodium ethanolate; N,N-diethylaniline hydrochloride; tin(IV) chloride; trichlorophosphate; In ethanol; acetic acid butyl ester; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1248/cpb.36.2673

Reference yield:

2,4,6-trichloro-5-hexyl-pyrimidine (14077-70-4) → C37H38N2O9 (120268-62-4)

Guidance literature:

Multi-step reaction with 4 steps

1: acetonitrile / 1 h

2: potassium tert-butoxide / 2 h / 75 °C

3: Raney Ni W-2 / ethanol / 3 h / Heating

4: 99 percent / stannic chloride / acetonitrile / Ambient temperature

With Raney Ni W-2; potassium tert-butylate; tin(IV) chloride; In ethanol; acetonitrile;

DOI:10.1248/cpb.36.2673

upstream raw materials:

1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose

5-Hexyl-2,4-dimethoxy-pyrimidine

diethyl 2-hexylmalonate

2,4,6-trichloro-5-hexyl-pyrimidine

Refernces