(R,R)-2,3,4-trimethyl-5-phenylthiazolinium iodide

Base Information

• Chemical Name: (R,R)-2,3,4-trimethyl-5-phenylthiazolinium iodide
• CAS No.: 1190228-09-1
• Molecular Formula: C₁₂H₁₆NS*I
• Molecular Weight: 333.236
• Mol file: 1190228-09-1.mol

Synonyms:(R,R)-2,3,4-trimethyl-5-phenylthiazolinium iodide

Chemical Property of (R,R)-2,3,4-trimethyl-5-phenylthiazolinium iodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of (R,R)-2,3,4-trimethyl-5-phenylthiazolinium iodide

There total 1 articles about (R,R)-2,3,4-trimethyl-5-phenylthiazolinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

(R,R)-2,4-dimethyl-5-phenyl-thiazoline (166107-69-3) + methyl iodide (74-88-4) → (R,R)-2,3,4-trimethyl-5-phenylthiazolinium iodide (1190228-09-1)

Guidance literature:

In acetonitrile; at 20 ℃; for 72h; Inert atmosphere;

DOI:10.1002/ejoc.200900514

Reference yield: 75.0%

(R,R)-2,3,4-trimethyl-5-phenylthiazolinium iodide (1190228-09-1) + methanesulfonyl chloride (124-63-0) → (R,R)-3,4-dimethyl-5-phenyl-2-[(Z)-(methylsulfonyl)methylidene]thiazolidine (1190228-22-8)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1002/ejoc.200900514

upstream raw materials:

(R,R)-2,4-dimethyl-5-phenyl-thiazoline

methyl iodide

Downstream raw materials:

(R,R)-3,4-dimethyl-5-phenyl-2-[(Z)-(methylsulfonyl)methylidene]thiazolidine

Refernces