Technology Process of C47H79NO11
There total 5 articles about C47H79NO11 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
1-O-palmitoyl-2-[(9z)-octadenoyl]-glycerol;
With
pyridine; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 0 ℃;
for 0.05h;
Inert atmosphere;
nitroveratryloxycarbonyl chloride;
In
dichloromethane;
at 20 ℃;
for 18h;
Darkness;
Inert atmosphere;
DOI:10.1002/anie.201301716
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 0.25 h / 20 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: iron(III) chloride hexahydrate / dichloromethane; methanol / 0.5 h / 20 °C / Inert atmosphere
3.1: N-ethyl-N,N-diisopropylamine; pyridine / dichloromethane / 0.05 h / 0 °C / Inert atmosphere
3.2: 18 h / 20 °C / Darkness; Inert atmosphere
With
pyridine; dmap; iron(III) chloride hexahydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
methanol; dichloromethane;
DOI:10.1002/anie.201301716
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: iron(III) chloride hexahydrate / dichloromethane; methanol / 0.5 h / 20 °C / Inert atmosphere
2.1: N-ethyl-N,N-diisopropylamine; pyridine / dichloromethane / 0.05 h / 0 °C / Inert atmosphere
2.2: 18 h / 20 °C / Darkness; Inert atmosphere
With
pyridine; iron(III) chloride hexahydrate; N-ethyl-N,N-diisopropylamine;
In
methanol; dichloromethane;
DOI:10.1002/anie.201301716
