Technology Process of C17H15NO3
There total 3 articles about C17H15NO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-Methyl-6-phenylbenzoxazole;
With
lithium hexamethyldisilazane;
In
tetrahydrofuran;
at -60 ℃;
for 0.5h;
Inert atmosphere;
Diethyl carbonate;
In
tetrahydrofuran;
for 0.5h;
Cooling with ice;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: acetic acid / 0.5 h / Reflux
2.1: potassium phosphate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 0.67 h / 150 °C / Inert atmosphere; Microwave irradiation
3.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -60 °C / Inert atmosphere
3.2: 0.5 h / Cooling with ice
With
potassium phosphate; acetic acid; lithium hexamethyldisilazane;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; 1,4-dioxane; water;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium phosphate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 0.67 h / 150 °C / Inert atmosphere; Microwave irradiation
2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -60 °C / Inert atmosphere
2.2: 0.5 h / Cooling with ice
With
potassium phosphate; lithium hexamethyldisilazane;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; 1,4-dioxane; water;