Technology Process of 3-(2-carboxymethylbenzylthio)benzyl bromide
There total 7 articles about 3-(2-carboxymethylbenzylthio)benzyl bromide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen bromide;
In
sulfolane;
at 15 ℃;
for 2.75h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium aluminum hydride / tetrahydrofuran / 1 h
2: dimethylformamide; H2O / 0.33 h / Ambient temperature
3: 93.2 percent / dry hydrogen bromide / tetrahydrothiophene 1,1-dioxide / 2.75 h / 15 °C
With
lithium aluminium tetrahydride; hydrogen bromide;
In
tetrahydrofuran; sulfolane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 85.6 percent / chlorosulfonic acid / 2 h / 120 - 125 °C
2: lithium aluminum hydride / tetrahydrofuran / 1 h
3: dimethylformamide; H2O / 0.33 h / Ambient temperature
4: 93.2 percent / dry hydrogen bromide / tetrahydrothiophene 1,1-dioxide / 2.75 h / 15 °C
With
chlorosulfonic acid; lithium aluminium tetrahydride; hydrogen bromide;
In
tetrahydrofuran; sulfolane; water; N,N-dimethyl-formamide;
