3,4-diaminophenylcarbamic acid isopropyl ester

Base Information

• Chemical Name: 3,4-diaminophenylcarbamic acid isopropyl ester
• CAS No.: 35198-67-5
• Molecular Formula: C₁₀H₁₅N₃O₂
• Molecular Weight: 209.248
• Mol file: 35198-67-5.mol

Synonyms:3,4-diaminophenylcarbamic acid isopropyl ester

Chemical Property of 3,4-diaminophenylcarbamic acid isopropyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 3,4-diaminophenylcarbamic acid isopropyl ester

There total 2 articles about 3,4-diaminophenylcarbamic acid isopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-isopropoxycarbonylamino-2-nitroaniline (30713-39-4) → 3,4-diaminophenylcarbamic acid isopropyl ester (35198-67-5)

Guidance literature:

With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; isopropyl alcohol; under 760 Torr; Ambient temperature;

Reference yield:

2-nitro-1,4-phenylenediamine (5307-14-2,183870-67-9) → 3,4-diaminophenylcarbamic acid isopropyl ester (35198-67-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 12 g / dimethylaniline / acetonitrile / 3 h / Ambient temperature

2: 6.5 g / H₂, HCl / 10percent Pd-C / methanol; propan-2-ol / 760 Torr / Ambient temperature

With hydrogenchloride; hydrogen; 2,3-Dimethylaniline; palladium on activated charcoal; In methanol; isopropyl alcohol; acetonitrile;

Reference yield:

1,3-thiazole-4-carbaldehyde (3364-80-5) + 3,4-diaminophenylcarbamic acid isopropyl ester (35198-67-5) → cambendazol (26097-80-3)

Guidance literature:

With sulfur; In xylene; for 8h; Heating;

upstream raw materials:

4-isopropoxycarbonylamino-2-nitroaniline

2-nitro-1,4-phenylenediamine

Downstream raw materials:

cambendazol

Refernces